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Discussion History

Structure and Composition

Assembly

A benchtop powder X-ray diffractometer with analysis software, a reference database and a silicon standard identifies the crystalline phases in a fired or melted sample. A stereo microscope, a density kit and an optional electron microscope check its microstructure and density. A full specification article for this item is being written. Meanwhile its bill of materials and connections are below.

Structure and Composition parts and their functions

8 top-level parts · 768 parts in total · full bill of materials below
Structure and Composition parts diagram: 1 x-ray diffractometer, 2 zero-background sample holders, 3 phase identification and rietveld software, 4 reference pattern database, 5 silicon powder line position standard, 6 stereo microscope, 7 density determination kit, 8 tabletop electron microscope. 768 parts in 8 top-level items.
Structure and Composition parts diagram. Numbers match the table below; each box is one top-level part or assembly with what it contains.
#PartQtyWhat it does
1 X-Ray Diffractometer 10 parts 1× Records the powder diffraction pattern of a ground sample so its crystalline phases can be identified and lattice parameters refined. Core
2 Zero-Background Sample Holders 4× Holds a few milligrams of powder in the diffractometer without adding substrate peaks or an amorphous hump to the pattern. Useful
3 Phase Identification and Rietveld Software 1× Matches a measured pattern against reference patterns to name the phases and refines lattice parameters and phase fractions by the Rietveld method. Core
4 Reference Pattern Database 1× Supplies the reference patterns and crystal structures that a measured diffraction pattern is matched against to name the phases. Core
5 Silicon Powder Line Position Standard 1× Calibrates the diffractometer's 2-theta scale, run alone or mixed into a sample, so the lattice parameters of a new phase can be trusted. Useful, 7.5 g
6 Stereo Microscope 8 parts 1× Magnifies pellets, arc-melted buttons and fracture surfaces for inspection and for placing four-probe contacts on small samples. Useful
7 Density Determination Kit 1× Weighs a pellet in air and immersed in a liquid on the analytical balance, giving its Archimedes density to compare with the X-ray density. Useful, kit
8 Tabletop Electron Microscope 5 parts 1× Images grain size, porosity and second phases at the micrometer scale and measures the elemental composition of each region by EDS. Optional

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Build & assembly graph

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Bill of materials for Structure and Composition

8 top-level lines · 117 rows shown · 768 parts total · indented to 3 levels
# Item / sub-assembly Part no. Qty/assy Ext. qty Parts Type
1 X-Ray Diffractometer 10 parts x-ray-diffractometer 1× 1 705 product
1.1 X-Ray Tube & Generator 4 parts xrd-tube-generator 1× 1 107 assembly
1.1.1 X-Ray Tube 3 parts + deeper › xrd-xray-tube 1× 1 3 assembly
1.1.2 High-Voltage Generator 5 parts + deeper › xrd-hv-generator 1× 1 102 assembly
1.1.3 Beam Shutter xrd-shutter 1× 1 · part
1.1.4 Tube Shield Housing xrd-tube-shield 1× 1 · part
1.2 Theta-Theta Goniometer 6 parts xrd-goniometer 1× 1 59 assembly
1.2.1 Theta Arm xrd-theta-arm 2× 2 · part
1.2.2 Goniometer Motor 4 parts + deeper › xrd-goniometer-motor 2× 2 24 assembly
1.2.3 Helical Gear Pair gear-pair 2× 2 · part
1.2.4 Optical Angle Encoder xrd-angle-encoder 2× 2 · part
1.2.5 Ball Bearing ball-bearing 4× 4 · part
1.2.6 Goniometer Base xrd-goniometer-base 1× 1 · part
1.3 Sample Stage 3 parts xrd-sample-stage 1× 1 25 assembly
1.3.1 Sample Spinner 2 parts + deeper › xrd-sample-spinner 1× 1 22 assembly
1.3.2 Sample Holder xrd-sample-holder 1× 1 · part
1.3.3 Ball Bearing ball-bearing 2× 2 · part
1.4 Strip Detector 5 parts xrd-detector 1× 1 64 assembly
1.4.1 Silicon Strip Sensor xrd-strip-sensor 1× 1 · part
1.4.2 Photon-Counting Readout ASIC xrd-readout-asic 1× 1 · part
1.4.3 CMOS Image Sensor image-sensor 1× 1 · part
1.4.4 Bare PCB pcb-bare 1× 1 · part
1.4.5 SMD Passive (R/C/L) smd-passives 60× 60 · part
1.5 Optics & Monochromator 5 parts xrd-optics 1× 1 6 assembly
1.5.1 Divergence Slit xrd-divergence-slit 1× 1 · part
1.5.2 Receiving Slit xrd-receiving-slit 1× 1 · part
1.5.3 Soller Slit xrd-soller-slit 2× 2 · part
1.5.4 Monochromator Crystal xrd-monochromator 1× 1 · part
1.5.5 Beta Filter xrd-beam-filter 1× 1 · part
1.6 Shielded Enclosure 5 parts xrd-enclosure 1× 1 13 assembly
1.6.1 Shield Panel xrd-shield-panel 4× 4 · part
1.6.2 Leaded Viewing Window xrd-leaded-window 1× 1 · part
1.6.3 Door Interlock Switch xrd-door-interlock 2× 2 · part
1.6.4 Relay relay 4× 4 · part
1.6.5 Fastener Set fastener-set 2× 2 · part
1.7 Control & Computer 5 parts xrd-control-computer 1× 1 384 assembly
1.7.1 Instrument Controller 5 parts + deeper › xrd-controller 1× 1 167 assembly
1.7.2 Control PC 4 parts + deeper › xrd-control-pc 1× 1 214 assembly
1.7.3 LCD Panel lcd-panel 1× 1 · part
1.7.4 Touch Digitizer touch-digitizer 1× 1 · part
1.7.5 Power Supply power-supply 1× 1 · part
1.8 Cooling System 2 parts xrd-cooling 1× 1 25 assembly
1.8.1 Recirculating Chiller 4 parts + deeper › xrd-chiller 1× 1 24 assembly
1.8.2 Blower Motor blower-motor 1× 1 · part
1.9 Wire Bundle wire-bundle 2× 2 · part
1.10 Connector connector 20× 20 · part
2 Zero-Background Sample Holders zero-background-sample-holders 4× 4 · part
3 Phase Identification and Rietveld Software phase-identification-and-rietveld-software 1× 1 · part
4 Reference Pattern Database reference-pattern-database 1× 1 · part
5 Silicon Powder Line Position Standard silicon-powder-line-position-standard 1× 1 · part
6 Stereo Microscope 8 parts stereo-microscope 1× 1 32 product
6.1 Stereo Optical Head 4 parts stereo-microscope-optical-head 1× 1 4 assembly
6.1.1 Left Zoom Lens Unit stereo-microscope-left-zoom 1× 1 · part
6.1.2 Right Zoom Lens Unit stereo-microscope-right-zoom 1× 1 · part
6.1.3 Common Objective Lens stereo-microscope-objective-lens 1× 1 · part
6.1.4 Beam Combiner Optics stereo-microscope-beam-combiner 1× 1 · part
6.2 Eyepiece Pair Assembly 3 parts stereo-microscope-eyepieces 2× 2 3 assembly
6.2.1 Left Eyepiece stereo-microscope-left-eyepiece 1× 2 · part
6.2.2 Right Eyepiece stereo-microscope-right-eyepiece 1× 2 · part
6.2.3 Eyepiece Tube Mount stereo-microscope-eyepiece-mount 1× 2 · part
6.3 Synchronized Zoom Body 3 parts stereo-microscope-zoom-body 1× 1 3 assembly
6.3.1 Zoom Drive Knob stereo-microscope-zoom-drive 1× 1 · part
6.3.2 Zoom Coupling Mechanism stereo-microscope-zoom-coupling 1× 1 · part
6.3.3 Magnification Scale stereo-microscope-magnification-scale 1× 1 · part
6.4 Focus Assembly 4 parts stereo-microscope-focus-mechanism 1× 1 4 assembly
6.4.1 Coarse Focus Knob stereo-microscope-coarse-focus-knob 1× 1 · part
6.4.2 Fine Focus Knob stereo-microscope-fine-focus-knob 1× 1 · part
6.4.3 Focus Rack / Pinion stereo-microscope-focus-rack 1× 1 · part
6.4.4 Fine-Focus Differential Screw stereo-microscope-focus-pinion 1× 1 · part
6.5 Sample Stage Assembly 3 parts stereo-microscope-stage 1× 1 3 assembly
6.5.1 Stage Plate stereo-microscope-stage-plate 1× 1 · part
6.5.2 Slide Clamp Assembly stereo-microscope-slide-clamp 1× 1 · part
6.5.3 Rotation Bearing stereo-microscope-rotation-bearing 1× 1 · part
6.6 Microscope Stand 4 parts stereo-microscope-stand 1× 1 5 assembly
6.6.1 Articulating Arm stereo-microscope-arm 1× 1 · part
6.6.2 Ball Joint / Bearing stereo-microscope-ball-joints 2× 2 · part
6.6.3 Weighted Base stereo-microscope-base-weight 1× 1 · part
6.6.4 Fixed Column stereo-microscope-column 1× 1 · part
6.7 Illumination System 4 parts stereo-microscope-illumination 1× 1 4 assembly
6.7.1 LED Ring Light stereo-microscope-led-ring 1× 1 · part
6.7.2 LED Brightness Controller stereo-microscope-led-driver 1× 1 · part
6.7.3 Diffusion Dome stereo-microscope-light-diffuser 1× 1 · part
6.7.4 Light Guide Fiber or Optics stereo-microscope-light-guide 1× 1 · part
6.8 Optics Mounting Frame 3 parts stereo-microscope-optics-mount 1× 1 3 assembly
6.8.1 Mount Frame stereo-microscope-mount-frame 1× 1 · part
6.8.2 Optical Component Holders stereo-microscope-component-holders 1× 1 · part
6.8.3 Fastener Set fastener-set 1× 1 · part
7 Density Determination Kit density-determination-kit 1× 1 · part
8 Tabletop Electron Microscope 5 parts tabletop-electron-microscope 1× 1 23 product
8.1 Electron Column 6 parts tabletop-electron-microscope-electron-column 1× 1 6 assembly
8.1.1 Electron Gun tabletop-electron-microscope-gun-assembly 1× 1 · part
8.1.2 Accelerating Anode tabletop-electron-microscope-accelerating-anode 1× 1 · part
8.1.3 Condenser Coil tabletop-electron-microscope-condenser-coil 1× 1 · part
8.1.4 Objective Lens tabletop-electron-microscope-objective-coil 1× 1 · part
8.1.5 Column Tube tabletop-electron-microscope-column-tube 1× 1 · part
8.1.6 HV Cable tabletop-electron-microscope-high-voltage-cable 1× 1 · part
8.2 Vacuum Pump Unit 5 parts tabletop-electron-microscope-vacuum-pump 1× 1 5 assembly
8.2.1 Turbomolecular Rotor tabletop-electron-microscope-turbo-rotor 1× 1 · part
8.2.2 Roughing Pump tabletop-electron-microscope-roughing-pump 1× 1 · part
8.2.3 Pump Controller tabletop-electron-microscope-pump-controller 1× 1 · part
8.2.4 Vacuum Gauge tabletop-electron-microscope-vacuum-gauge 1× 1 · part
8.2.5 Isolation Valve tabletop-electron-microscope-isolation-valve 1× 1 · part
8.3 Specimen Chamber 4 parts tabletop-electron-microscope-specimen-chamber 1× 1 4 assembly
8.3.1 Motorized Stage tabletop-electron-microscope-motorized-stage 1× 1 · part
8.3.2 Specimen Clip tabletop-electron-microscope-specimen-clip 1× 1 · part
8.3.3 BSE Scintillator tabletop-electron-microscope-bse-scintillator 1× 1 · part
8.3.4 Chamber Housing tabletop-electron-microscope-chamber-housing 1× 1 · part
8.4 Control Electronics Box 5 parts tabletop-electron-microscope-control-box 1× 1 5 assembly
8.4.1 Scan Generator tabletop-electron-microscope-scan-circuit 1× 1 · part
8.4.2 Detector Amp tabletop-electron-microscope-detector-amp 1× 1 · part
8.4.3 HV Supply tabletop-electron-microscope-high-voltage-supply 1× 1 · part
8.4.4 Interface Board tabletop-electron-microscope-interface-board 1× 1 · part
8.4.5 Display Module tabletop-electron-microscope-display-module 1× 1 · part
8.5 Cooling Unit 3 parts tabletop-electron-microscope-cooling-unit 1× 1 3 assembly
8.5.1 Mini Pump tabletop-electron-microscope-mini-pump 1× 1 · part
8.5.2 Mini Radiator tabletop-electron-microscope-mini-radiator 1× 1 · part
8.5.3 Coolant Loop tabletop-electron-microscope-coolant-loop 1× 1 · part

Where the structure and composition is used

1 product across 1 domain contain it, directly or inside a sub-assembly

Used in 1 assembly

Sourcing: possible vendors

Browse the supplier directory → Prices, MOQ, and lead times are algorithmic estimates, not quotes, and not claims about these companies. Company mappings are curated by keyword; est. price band $0.50–$200. How estimates work
VendorHQSpecialtyMOQLead time
🇮🇳Bharat Forge
bharatforge.com ↗
Pune, IN Forgings & metal parts 500 pcs 6–10 wks
dicastal.com ↗ Qinhuangdao, CN Aluminium castings & wheels 500 pcs 6–10 wks
tataautocomp.com ↗ Pune, IN Auto components 500 pcs 6–10 wks
🇸🇬Beyonics
beyonics.com ↗
Singapore Precision metal & mfg 500 pcs 6–10 wks
sundaram-clayton.com ↗ Chennai, IN Die castings 500 pcs 6–10 wks